Olive mill wastewaterevaporation ponds long term stored ...
The samples were airdried at 45 °C to avoid the phenolic compounds degradation, ground to obtain a dust particle size with vibratory ball mill (Frischt Pulverisette SPARTAN), and left at 105 °C to constant weight before chemical analysis. Fresh subsamples stored at 4 °C were used for the analysis of phytotoxicity and ecotoxicity.